Ultrafast chiral separations for high throughput enantiopurity analysis CL Barhate, LA Joyce, AA Makarov, K Zawatzky, F Bernardoni, ... Chemical communications 53 (3), 509-512, 2017 | 148 | 2017 |
Ultrafast chiral chromatography as the second dimension in two-dimensional liquid chromatography experiments CL Barhate, EL Regalado, ND Contrella, J Lee, J Jo, AA Makarov, ... Analytical chemistry 89 (6), 3545-3553, 2017 | 136 | 2017 |
Current challenges and future prospects in chromatographic method development for pharmaceutical research FT Mattrey, AA Makarov, EL Regalado, F Bernardoni, M Figus, MB Hicks, ... TrAC Trends in Analytical Chemistry 95, 36-46, 2017 | 114 | 2017 |
Chromatographic resolution of closely related species in pharmaceutical chemistry: dehalogenation impurities and mixtures of halogen isomers EL Regalado, P Zhuang, Y Chen, AA Makarov, WA Schafer, N McGachy, ... Analytical chemistry 86 (1), 805-813, 2014 | 68 | 2014 |
Chaotropic effects in sub/supercritical fluid chromatography via ammonium hydroxide in water-rich modifiers: enabling separation of peptides and highly polar pharmaceuticals at … J Liu, AA Makarov, R Bennett, IA Haidar Ahmad, J DaSilva, M Reibarkh, ... Analytical chemistry 91 (21), 13907-13915, 2019 | 60 | 2019 |
The emergence of universal chromatographic methods in the research and development of new drug substances EL Regalado, IA Haidar Ahmad, R Bennett, V D’Atri, AA Makarov, ... Accounts of chemical research 52 (7), 1990-2002, 2019 | 53 | 2019 |
Macrocyclic glycopeptide chiral selectors bonded to core-shell particles enables enantiopurity analysis of the entire verubecestat synthetic route CL Barhate, DA Lopez, AA Makarov, X Bu, WJ Morris, A Lekhal, ... Journal of Chromatography A 1539, 87-92, 2018 | 53 | 2018 |
pKa measurements for the SAMPL6 prediction challenge for a set of kinase inhibitor-like fragments M Işık, D Levorse, AS Rustenburg, IE Ndukwe, H Wang, X Wang, ... Journal of computer-aided molecular design 32, 1117-1138, 2018 | 48 | 2018 |
Evaluation of global conformational changes in peptides and proteins following purification by supercritical fluid chromatography NM Schiavone, R Bennett, MB Hicks, GF Pirrone, EL Regalado, I Mangion, ... Journal of Chromatography B 1110, 94-100, 2019 | 41 | 2019 |
Search for improved fluorinated stationary phases for separation of fluorine-containing pharmaceuticals from their desfluoro analogs EL Regalado, AA Makarov, R McClain, M Przybyciel, CJ Welch Journal of Chromatography A 1380, 45-54, 2015 | 38 | 2015 |
Multi-column ultra-high performance liquid chromatography screening with chaotropic agents and computer-assisted separation modeling enables process development of new drug … IAH Ahmad, W Chen, HM Halsey, A Klapars, J Limanto, GF Pirrone, ... Analyst 144 (9), 2872-2880, 2019 | 35 | 2019 |
Supercritical fluid chromatography-photodiode array detection-electrospray ionization mass spectrometry as a framework for impurity fate mapping in the development and … GF Pirrone, RM Mathew, AA Makarov, F Bernardoni, A Klapars, ... Journal of Chromatography B 1080, 42-49, 2018 | 33 | 2018 |
Liophilic mobile phase additives in reversed phase HPLC A Makarov, R LoBrutto, Y Kazakevich Journal of Liquid Chromatography & Related Technologies® 31 (11-12), 1533-1567, 2008 | 33 | 2008 |
Enantioselective UHPLC Screening Combined with In Silico Modeling for Streamlined Development of Ultrafast Enantiopurity Assays GL Losacco, H Wang, IA Haidar Ahmad, J DaSilva, AA Makarov, ... Analytical Chemistry 94 (3), 1804-1812, 2021 | 29 | 2021 |
Generic anion-exchange chromatography method for analytical and preparative separation of nucleotides in the development and manufacture of drug substances FR Tsay, IAH Ahmad, D Henderson, N Schiavone, Z Liu, AA Makarov, ... Journal of Chromatography A 1587, 129-135, 2019 | 29 | 2019 |
Investigation of the effect of pressure and liophilic mobile phase additives on retention of small molecules and proteins using reversed-phase ultrahigh pressure liquid … A Makarov, R LoBrutto, P Karpinski, Y Kazakevich, C Christodoulatos, ... Journal of liquid chromatography & related technologies 35 (3), 407-427, 2012 | 26 | 2012 |
Association of Bacillus firmus E3 and Klebsiella terrigena E6 with increased ability for nitrogen fixation AK Zlotnikov, YN Shapovalova, AA Makarov Soil Biology and Biochemistry 33 (11), 1525-1530, 2001 | 25 | 2001 |
Use of MALDI-MS combined with differential hydrogen–deuterium exchange for semiautomated protein global conformational screening GF Pirrone, H Wang, N Canfield, AS Chin, TA Rhodes, AA Makarov Analytical Chemistry 89 (16), 8351-8357, 2017 | 24 | 2017 |
Unusual reversal of enantioselectivity in the asymmetric autocatalysis of pyrimidyl alkanol triggered by chiral aromatic alkanols and amines A Matusmoto, S Fujiwara, Y Hiyoshi, K Zawatzky, AA Makarov, CJ Welch, ... Organic & Biomolecular Chemistry 15 (3), 555-558, 2017 | 23 | 2017 |
A chemoenzymatic strategy for site-selective functionalization of native peptides and proteins A Fryszkowska, C An, O Alvizo, G Banerjee, KA Canada, Y Cao, ... Science 376 (6599), 1321-1327, 2022 | 20 | 2022 |